CHEMISTRY 260 – Analytical Chemistry
Spring 2002
Dr. Victor Lau (URL: www.oocities.org/thinkertank)
Office: Harney 406 Telephone:
666-6400 e-mail: lauv@usfca.edu
Class Meetings:Lecture Tuesday, Thursday 12:10 pm - 1:00 pm Harney 510
Lab Tuesday, Thursday
or, Tuesday,
Thursday
Office Hours: Tuesday and Thursday: 1000-1130; 1430-1630
Textbook: Daniel C. Harris, Exploring
Chemical Analysis; 2nd Edition W. H. Freeman:
Also Required: Duplicate-page lab notebook. (Should be right next to the text in the bookstore.)
References: useful sources of fresh explanations and extra problems (in SAACS room)
1. Contemporary Chemical Analysis (1998), by J. F. Rubinson and K. A. Rubinson.
2. Quantitative Chemical Analysis, 4th Ed. (1995), by D. C. Harris.
3. Fundamentals of Analytical Chemistry (1988), by Skoog, West, and Holler.
Homework: Throughout the term text problems will be suggested and extra problem sets may be given out. These are crucial for the development of your understanding, but in general they will not be collected or graded, unless otherwise specified.
Exams: There will be three midterm exams and a final examination:
Exam 1 |
Tuesday |
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Exam 2 |
Tuesday |
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Exam 3 |
Tuesday |
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Final Exam |
To Be Determined |
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No Makeup Exams will be GIVEN
EXAM REGRADES: Requests for re-grades must be turned in to
the instructor by the end of the first class after the exams have been given
back to the students. On the front of
the exam, specify which problem you would like re-graded. Re-grade requests involving fewer than five
points will not be considered. Also,
keep in mind that any test submitted for re-grading may be re-graded in its
entirety.
Grading: The course grade will be determined as follows:
Three midterm exams |
30% |
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Final exam |
30% |
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Class/Lab participation |
5% |
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Lab reports |
35% |
Lab Policies: NO MAKE-UP LABS WILL BE PERMITTED.
Except when specifically instructed
otherwise, students must complete all labwork within
their designated lab periods. This means
that students are expected to show up for lab on time. It also means they must leave by the
scheduled end of the period. When
working in groups, all members of a group should attempt to make roughly equal contributions
in terms of time and effort. If a
student consistently shows up late for lab, his/her lab grade will be lowered
accordingly. If a student accumulates
excessive unexcused absences from the lab, he/she will be required to drop the
course.
CHEMISTRY 260 –– Spring 2002 Tentative Schedule
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1 |
Tues 1/22 Thur 1/24 |
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No lab class |
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2 |
Tues 1/29 Thur 1/31 |
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Statistical Analysis of Indicators Statistical Analysis of Indicators |
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3 |
Tues 2/5 Thur 2/7 |
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UV Detn of a Mixture of Vanillin UV Detn of a Mixture of
Vanillin |
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4 |
Tues 2/12 Thur 2/14 |
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UV Determination of a
Mixture of Metal Ions |
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5 |
Tues 2/19 Thur 2/21 |
EXAM 1 |
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6 |
Tues 2/26 Thur 2/28 |
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Round Robin consisting of 3 experiments: 1.
GC Determination of Ethanol in Beer 2.
Computer Stimulation of HPLC 3. HPLC Analysis of Urinary Compounds |
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7 |
Tues 3/5 Thur 3/7 |
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8 |
Tues 3/12 Thur 3/14 |
Ch. 7-9: Acid-Base Equilibria,
Titrations |
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9 |
Tues 3/19 Thur 3/21 |
Ch. 7-9: Acid-Base Equilibria,
Titrations Review |
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10 |
Tues 3/26 Thur 3/28 |
SPRING RECESS |
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11 |
Tues 4/2 Thur 4/4 |
EXAM 2 |
Characterization of Weak Acids |
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12 |
Tues 4/9 Thur 4/11 |
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13 |
Tues 4/16 Thur 4/18 |
Ch. 13-16: Electrochemistry Ch. 13-16: Electrochemistry |
Tartaric Acid Content in Wine |
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14 |
Tues 4/23 Thur 4/25 |
Ch. 13-16: Electrochemistry Ch. 13-16: Electrochemistry |
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15 |
Tues 4/30 Thur 5/2 |
EXAM 3 |
Potentiometric Determination of Chloride Ion |
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16 |
Tues 5/7 Thur 5/9 |
Review Review |
Check Out |